Boc-4-Piperidinecarboxylic Acid, 1-
1-boc-piperidine-4-carboxylic acid
CAS: 84358-13-4;174316-71-3
Molecular Formula: C11H19NO4
Boc-4-Piperidinecarboxylic Acid, 1- - Names and Identifiers
Boc-4-Piperidinecarboxylic Acid, 1- - Physico-chemical Properties
| Molecular Formula | C11H19NO4 |
| Molar Mass | 229.27 |
| Density | 1.164±0.06 g/cm3(Predicted) |
| Melting Point | 148-153°C |
| Boling Point | 353.2°C at 760 mmHg |
| Flash Point | 167.4°C |
| Water Solubility | Insoluble in water. |
| Vapor Presure | 6.15E-06mmHg at 25°C |
| Appearance | White Crystalline Powder |
| pKa | 4.56±0.20(Predicted) |
| Storage Condition | Keep in dark place,Sealed in dry,Room Temperature |
| MDL | MFCD00076999 |
Boc-4-Piperidinecarboxylic Acid, 1- - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | R36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S37/39 - Wear suitable gloves and eye/face protection |
| WGK Germany | 3 |
| HS Code | 29339900 |
| Hazard Class | IRRITANT |
Boc-4-Piperidinecarboxylic Acid, 1- - Upstream Downstream Industry
Boc-4-Piperidinecarboxylic Acid, 1- - Production method
Open Data Unverified Data
| 4-picolinic acid (1g, 7.74mmol) is dissolved in NaOH solution (2 M,10 mL), THF (10 mL) solution dissolved with BOC anhydride (2.53g, 11.61mmol) is slowly added under ice bath condition, the reaction is stirred at room temperature for 1 hour, THF is removed by rotary evaporator, the pH value of aqueous phase is adjusted to 5-6 with dilute hydrochloric acid, and then extracted with ethyl acetate, the combined organic phase was dried and filtered with anhydrous Na2SO4, and the filtrate was concentrated with a rotary evaporator. After vacuum drying, the white solid compound 1-Boc-4-piperidinic acid (1.78g, 7.76mmol, yield 100%) was obtained. |
Last Update：2024-04-09 19:43:38
Boc-4-Piperidinecarboxylic Acid, 1- - Introduction
1-Boc-4-piperidinic acid is a white solid compound, which can be prepared from 4-picolinic acid by reacting with Boc acid anhydride.
Last Update：2024-04-09 20:52:54
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View History
Raw Materials for Boc-4-Piperidinecarboxylic Acid, 1-
Downstream Products for Boc-4-Piperidinecarboxylic Acid, 1-
tert-butyl 4-(1H-benzo[d]iMidazol-2-yl)piperidine-1-carboxylate
1-BOC-PIPERIDIN-4-YLPROPIONIC ACID
1-Boc-4-[methoxy(methyl)carbamoyl]piperidine
tert-butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)piperidine-1-carboxylate
N-TERT-BUTOXYCARBONYL-4-(4-TOLUENESULFONYLOXYMETHYL)PIPERIDINE
1-(PIPERIDIN-4-YLCARBONYL)PIPERIDINE
1-BOC-PIPERIDIN-4-YLPROPIONIC ACID
1-Boc-4-[methoxy(methyl)carbamoyl]piperidine
tert-butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)piperidine-1-carboxylate
N-TERT-BUTOXYCARBONYL-4-(4-TOLUENESULFONYLOXYMETHYL)PIPERIDINE
1-(PIPERIDIN-4-YLCARBONYL)PIPERIDINE